Inorganic chemicals for industrical usePreparations of standard and reagent solutions for chemical analysisPart 2: Preparations of standard solutions for impurity
1 Scope
This part specifies the methods of preparing standard solutions for impurity for chemical analysis of inorganic chemicals for industrial use.
It applies to the preparation of standard solution containing exact amount of certain element, ion or molecule in certain volume required for the determination of impurities in analysis of inorganic chemicals for industrial use. It may also be used for chemical analysis of other chemical products for industrial use.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated references, only the dated edition is applicable to this document. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 6682-2008 Water for analytical laboratory use - Specification and test methods
HG/T 3696.1 Inorganic chemicals for industrial use - Preparations of standard and reagent solutions for chemical analysis - Part 1: Preparations of standard volumetric solutions
HG/T 3696.3 Inorganic chemicals for industrial use - Preparations of standard and reagent solutions for chemical analysis - Part 3: Preparations of reagent solutions
3 General requirements
3.1 Unless otherwise specified, the water adopted in this part refers to Grade 3 water specified in GB/T 6682-2008.
3.2 The purity of any reagent used in this part is above analytically pure. Surface treatment shall be conducted before applying easily oxidized metals.
3.3 Unless otherwise specified, the required standard and reagent solutions in annexes of this part are prepared in accordance with HG/T 3696.1 and HG/T 3696.3.
3.4 In diluting standard solutions for impurity, accurate measuring instruments (pipette and volumetric flask) shall be used for integral multiple dilution, and the volume of standard solution measured each time shall not be less than 1.00mL.
Foreword i
1 Scope
2 Normative references
3 General requirements
4 Warning
5 Preparation methods
Annex A (Informative) Calibration of standard solutions for sulfur impurity
Annex B (Normative) Methods for determining the contents of two solutions
Annex C (Informative) Method of preparing standard solutions for impurity calculated by organic molecule