标准编号:	GB/T 39560.10-2024
中文名称:	电子电气产品中某些物质的测定 第10部分：气相色谱-质谱法（GC-MS）测定聚合物和电子件中的多环芳烃（PAHs）
英文名称:	Determination of certain substances in electrical and electronic products—Part 10:Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS)
中标分类:	L10    电子元件综合
行业分类:	GB    国家标准
发布机构:	国家市场监督管理总局;国家标准化管理委员会
发布日期:	2024-8-23
实施日期:	2024-12-1
标准状态:	valid
翻译语言:	英文
文件格式:	PDF
翻译字数:	38000 字
交付时间:	1~3 个工作日

GB/T 39560.10-2024 Determination of certain substances in electrical and electronic products - Part 10: Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS) 1 Scope This document specifies one normative technique for the determination of polycyclic aromatic hydrocarbons (PAHs) in polymers of electrotechnical products. These PAHs can especially be found in the plastic and rubber parts of a wide range of consumer articles. They are present as impurities in some of the raw materials used in the production of such articles, in particular in extender oils and in carbon black. They are not added intentionally to the articles and do not perform any specific function as constituents of the plastic or rubber parts. The gas chromatography-mass spectrometry (GC-MS) test method is suitable for the determination of polycyclic aromatic hydrocarbons (PAHs). These test methods have been evaluated for use with plastics and rubbers. These test methods have been evaluated for use with ABS (acrylonitrile butadiene styrene) containing individual PAHs ranging from 37.2 mg/kg to 119 mg/kg and rubbers containing individual PAHs ranging from 1 mg/kg to 221.2 mg/kg. 2 Normative references The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. GB/T 39560.1-2020 Determination of certain substances in electrotechnical products - Part 1: Introduction and overview ISO 3696 Water for analytical laboratory use - Specification and test methods 3 Terms, definitions and abbreviated terms 3.1 Terms and definitions No terms and definitions are listed in this document. ISO and IEC maintain terminological databases for use in standardization at the following addresses: ——IEC Electropedia: available at http://www.electropedia.org/ ——ISO Online browsing platform: available at http://www.iso.org/obp 3.2 Abbreviated terms ABS: acrylonitrile butadiene styrene CCC: continuing calibration check standard EI: electron ionization GC-MS: gas chromatography-mass spectrometry IS: internal standard IUPAC: International Union of Pure and Applied Chemistry LOD: limit of detection LOQ: limit of quantification MDL: method detection limit PAH: polycyclic aromatic hydrocarbon PBDE: polybrominated diphenyl ether QC: quality control RSD: relative standard deviation SIM: selected ion monitoring TICS: tentatively identified compounds 4 Principle PAH compounds are quantitatively determined using ultrasonic extraction or Soxhlet extraction followed by gas chromatography-mass spectrometry (GC-MS) using single (or "selected") ion monitoring (SIM).