This standard specifies the qualitative analysis and quantitative analysis for the phase composition of various polycrystalline materials with polycrystal X-ray diffractometer under room temperature, high and low temperature, the determination of granular size (about 1~200nm) and intragranular lattice distortion and the general determination method for the lattice constant of crystals in cubic system.
This standard is applicable to various polycrystal materials, like metal, alloy, mineral, soil, ceramic, building material, organic and inorganic compound, medicine, polymer and environmentally-friendly specimen. It is primarily applicable to diffractometer method. However, photographic method may be applied by reference.
Foreword I
1. Scope
2. Normative References
3. Definitions
4. Method Principle
5. Reagent and Material
6. Instrument
7. Specimen
8. Analysis Procedure
9. Expression of Analysis Result
10. Safety Precautions
Appendix A (Normative) Calibration of Diffraction Peak Position (2θ)
Appendix B (Normative) Experimental Data Record
Appendix C (Informative) Description for PDF
Appendix D (Informative) References
Appendix E (Informative) Various Standard Material and Standard Data
Appendix F (Informative) Experimental Data and Record Format for Phase Qualitative Analysis of X-ray
Appendix G (Informative) Sign of Ionizing Radiation
